Temperature effect on calcium phosphate synthesized from chicken eggshells and ammonium phosphate

บทความในวารสาร

ผู้เขียน/บรรณาธิการ

กลุ่มสาขาการวิจัยเชิงกลยุทธ์

ไม่พบข้อมูลที่เกี่ยวข้อง

รายละเอียดสำหรับงานพิมพ์

รายชื่อผู้แต่ง: Pankaew P., Hoonnivathana E., Limsuwan P., Naemchanthara K.

ผู้เผยแพร่: Asian Network for Scientific Information (ANSINET)

ปีที่เผยแพร่ (ค.ศ.): 2010

วารสาร: Journal of Applied Sciences (1812-5654)

Volume number: 10

Issue number: 24

หน้าแรก: 3337

หน้าสุดท้าย: 3342

จำนวนหน้า: 6

นอก: 1812-5654

eISSN: 1812-5662

URL: https://www.scopus.com/inward/record.uri?eid=2-s2.0-78049406676&doi=10.3923%2fjas.2010.3337.3342&partnerID=40&md5=71c8686fdc46ec748d4d2e747035b58e

ภาษา: English-Great Britain (EN-GB)

ดูบนเว็บไซต์ของสำนักพิมพ์

บทคัดย่อ

Calcium phosphate ceramics such as hydroxyapatite (HAp, Ca10 (PO4)6 (OH)2) and [3-tricalcium phosphate ([3-TCP, Ca3 (PO4)2) are a high potential candidate for hard tissue implants in orthopedic and dental surgeries due to their chemical and structural similarity to bone minerals. Material that shows hydroxyapatite and [3-tricalcium phosphate phases is called Biphasic Calcium Phosphate (BCP). In present study, biphasic calcium phosphate was prepared and characterized for future applications on the utilization of bioactivity of HAp and resorbability of [3-TCP properties. It was simply synthesized by precipitation method using eggshell as the calcium source (Ca) in the form of calcium nitrate and ammonium phosphate as the phosphate source (P) to obtain biphasic calcium phosphate. The prepared BCP powders and crystal structure were characterized by X-Ray Diffraction (XRD), Rietveld refinements and Fourier transform infrared (FT-IR) techniques. The results indicate that BCP was observed at the calcining temperature of 700ฐC and above. Furthermore, the crystallinity of BCP increases with increasing temperature from 700-1200ฐC. The phase fractions of [3-TCP in the temperature range of 700-1200ฐC was found to be 10,17,18,19, 22 and 23 wt.%, respectively. The formation of BCP may arise from its non-stoichiometric composition of materials or a variation of synthesis parameters. ฉ 2010 Asian Network for Scientific Information.

คำสำคัญ

Chickeneggshell, Tricalcium phosphate