Effects of preparation parameters on morphology of cellulose nanowhiskers

Conference proceedings article

ผู้เขียน/บรรณาธิการ

กลุ่มสาขาการวิจัยเชิงกลยุทธ์

ไม่พบข้อมูลที่เกี่ยวข้อง

รายละเอียดสำหรับงานพิมพ์

รายชื่อผู้แต่ง: Phanwiroj P., Tanpichai S., Potiyaraj P.

ผู้เผยแพร่: Trans Tech Publications

ปีที่เผยแพร่ (ค.ศ.): 2014

Volume number: 1044-1045

หน้าแรก: 35

หน้าสุดท้าย: 38

จำนวนหน้า: 4

ISBN: 9783038352778

นอก: 1022-6680

eISSN: 1662-8985

URL: https://www.scopus.com/inward/record.uri?eid=2-s2.0-84922032415&doi=10.4028%2fwww.scientific.net%2fAMR.1044-1045.35&partnerID=40&md5=48ecedd8e91df3628a68621244ffca04

ภาษา: English-Great Britain (EN-GB)

ดูบนเว็บไซต์ของสำนักพิมพ์

บทคัดย่อ

The aim of this research was to study the parameters on the properties of cellulose nanowhiskers. Cellulose nanowhiskers were prepared from two different cellulose sources (filter paper and alpha cellulose), and their morphology were further investigated. Cellulose nanowhiskers were firstly extracted from two commercial cellulose sources (paper filter and alpha cellulose) using sulfuric treatement with treatment times of 20, 45, 70, 95 and 120 min respectively and temperature of 37, 45 and 60 ฐC respectively. The hydrolyzed cellulose was then neutralized with two different techniques, dialysis and titration. The samples were subsequently sonicated, and freezed dried. The effect of preparation conditions on the morphology of cellulose nanowhiskers was investigated. Cellulose nanowhiskers were characterized using scanning electron microscopy and transmission electron microscopy. The results showed that 9 nm diameter cellulose nanowhiskers can be prepared. A possible correlation between the preparation conditions and cellulose particle sizes could not be observed, but the titration process used to neutralize cellulose can shorten the length of the preparation time from 168 h to only 50 h. ฉ (2014) Trans Tech Publications, Switzerland.

คำสำคัญ

Cellulose nanowhisker, Neutralization technique